Hendershott, James P. "Am. Ind. Hyg. Assoc. J." 1986, 47(12) 742-746 ....Title: The Simultaneous Determination of Chloroformates and Phosgene at Low Concentrations in Air Using a Solid Sorbent Sampling - Gas Chromatographic Procedure. ...Collection: 350 mg XAD-2 coated with di-n-butylamine (explained in article) Since they say it can be used for phosgene possibly the HMP coated XAD-2 would work. ...Flowrate: 50 mL/min Volume 24 Liters Desorb with 2mL of Hexane, remove as much as possible from resin, add 1mL of 1N HCL. ...Analysis: GC/FID nothing special ...Keywords: Acid Chlorides; Chlorothioformates
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